By D.R. UHLMANN and N.J. KREIDL (Eds.)

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For instance, in Fig. (8) S's. EXAFS measurements then suggest that irreversible photostructural effects in a-As 2 S 3 films involve the breaking of homopolar (As-As) bonds and the generation of heteropolar (As-S) bonds. Similar observations have been reported by Nemanich on thermal annealing of a-As 2 S 3 films and both processes are envisaged in terms of the depolymerization of As 4 S 4 molecular units. Reversible photostructural effects in a-As 2 S 3 are more subtle. They can be detected in the annealed glass beyond the first coordination sphere.

1973). Crystalline and amorphous GeSe 2 and GeS have been studied by Oyanagi and coworkers (1981) using germanium K-edge EXAFS. While a-GeS 2 appears to have a 4:2 coordination arrangement like a-GeSe2, germanium is reported to be threefold coordinated in a-GeS—realizing a prediction made by Bienenstock on the basis of conventional X-ray diffraction measurements (1973). Fuoss and colleagues came to the same conclusions for a-GeSe in their anomalous dispersion studies. Interestingly, c-GeS and c-GeSe have distorted rock-salt structures, characterized by extensive mesomeric bonding arrangements.

Hence, by suitable choice of the angular position of the incident beam surface, specific structural information can be obtained. This will come from the first atomic layers for an angle of incidence less than the critical angle or from a surface region which may be over a /mi thick in the case of an angle above the critical angle. Referring back to Fig. 4, both the reflected beam, 7R, and the fluorescence signal, 7F, carry information about the X-ray absorption at the surface. ) Equation 10 ceases to hold for cj) ^ 0C because of an increasing contribution to R from the real part of the refractive index.

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